Feed reference materials in the system of metrological support of agro-industrial complex laboratories
https://doi.org/10.20915/2687-0886-2021-17-1-5-20
Abstract
The authors provided information about the developed matrix feed reference materials, certified for quality, nutritional value and toxicological contamination indicators for metrological support of analytical work in the article to confirm the compliance of products with requirements of national standards. Information on the stages of development of feed reference materials (selection and preparation of reference material, studies of heterogeneity and stability of feed reference material) is presented. There are demonstrated the results of reference materials certification according to certified indicators, their correctness confirmed by the results of thirty accredited laboratories.
The developed reference material of sunflower meal is registered in the State Register of approved types of reference materials under the number GSO 11612-2020. Reference materials of the composition of toasted soybean feed meal and complete feed for poultry (broilers) are approved as Industry-Specific by the Ministry of Agriculture of the Russian Federation (Department of Plant Production, Mechanization, Chemicalization and Plant Protection).
Feed reference materials are intended for metrological support of agro-industrial complex laboratories.
About the Authors
G. A. StupakovaRussian Federation
Galina A. Stupakova - PhD (Biology), head of the laboratory of metrological support of agroecological monitoring, All-Russian Research Institute of Agrochemistry.
31a Pryanishnikova St., Moscow, 127434.
S. A. Dengina
Russian Federation
Svetlana A. Dengina - senior researcher of the laboratory of metrological support of agroecological monitoring, All-Russian Research Institute of Agrochemistry.
31a Pryanishnikova St., Moscow, 127434.
E. E. Ignatyeva
Russian Federation
Elena E. Ignatyeva - senior researcher of the laboratory of metrological support of agroecological monitoring, All-Russian Research Institute of Agrochemistry.
31a Pryanishnikova St., Moscow, 127434.
T. I. Shchipletsova
Russian Federation
Tatiana I. Shchipletsova - senior researcher of the laboratory of metrological support of agroecological monitoring, All-Russian Research Institute of Agrochemistry.
31a Pryanishnikova St., Moscow, 127434.
D. K. Mitrofanov
Russian Federation
Dmitriy K. Mitrofanov - senior researcher of the laboratory of metrological support of agroecological monitoring, All-Russian Research Institute of Agrochemistry.
31a Pryanishnikova St., Moscow, 127434.
References
1. Davydova S. A. Food production as a factor of livestock breeding development in the current economical conditions. Journal of VNIIMZH. 2018;(3):139-142.
2. Bastov D. V. Perspektivy razvitiia mirovogo kormoproizvodstva [Prospects for the development of world feed production]. Agrarnik. 2013;(10):20-22.
3. Osnovy ekspertizy kormov i kormovykh dobavok [Osnovy ekspertizy kormov i kormovykh dobavok]. In: Informatsionnyi nekommercheskii resurs agro-archive.ru [Information non-commercial resource agro-archive.ru]. Available from: https://www.gov.uk/government/publications/living-well-withdementia-strategy [Accessed 20 January 2021].
4. Stupakova G. A., Ignat'eva E. E., Pankratova K. G., Den'gina S. A., Gromova T. B., Shchelokov V. I. et all. Metrological support of agrochemical laboratories in agroecological monitoring. Measurement Standards. Reference Materials. 2015;(3):71-79. (In Russ.).
5. Nalobin D. P., Osintseva E. V. Methods of establishing traceability of certified values of certified reference materials. Reference Materials. 2008;(2):16-26. (In Russ.)
6. Stupakova G. A., Lunev M. I., Dengina S. A. Reference samples for the quality evaluation and safety assessment of plant products. International agricultural journal. 2020;(3):60-65. http://dx.doi.org/10.24411/2587-6740-2020-13052.
7. Dengina S. A., Stupakova G. A., Ivanova V. M., Ilyushenko I. V. Reference standards of plant products with high content of-toxic elements. Plodorodie. 2018;(4):59-60.
8. Stupakova G. A., Ignatyeva E. E., Pankratova K. G., Den'gina S. A., Shhelokov V. I., Schipletsova T. I., Mitrofanov D. K. Activity of the pryanishnikov research institute of agricultural chemistry within the state service of certified reference materials. Plodorodie. 2018;(2):14-16.
9. GOST 13496.0-2016 Compound feeds, feed raw materials. Methods of sampling. Moscow: Standartinform Publ.; 2020. 13 p.
10. GOST 13979.0-86 Oilcakes, oilmeals and powdered mustard seed cake. Acceptance rules and methods of sampling. Moscow: IPK Izdatel'stvo standartov; 2002. 5 p.
11. GOST 8.531-2002 State system for ensuring the uniformity of measurements. Reference materials of composition of solid and disperse materials. Ways of homogeneity assessment. Moscow: IPK Izdatel'stvo standartov; 2003. 12 p.
12. GOST 8.532-2002 State system for ensuring the uniformity of measurements. Certified reference materials of composition of substances and materials. Interlaboratory metrological certification. Content and order of works. Moscow: IPK Izdatel'stvo standartov; 2003. 10 p.
13. GOST ISO/IEC 17025-2019 General requirements for the competence of testing and calibration laboratories. Moscow: Standartinform Publ.; 2020. 13 p.
Review
For citations:
Stupakova G.A., Dengina S.A., Ignatyeva E.E., Shchipletsova T.I., Mitrofanov D.K. Feed reference materials in the system of metrological support of agro-industrial complex laboratories. Measurement Standards. Reference Materials. 2021;17(1):5-20. (In Russ.) https://doi.org/10.20915/2687-0886-2021-17-1-5-20

This work is licensed under a Creative Commons Attribution-NonCommercial 4.0 International (CC BY-NC 4.0).