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Interlaboratory comparisons on determining of alcohol by volume (abv) in vodka Measurement standards

https://doi.org/10.20915/2687-0886-2020-16-1-57-66

Abstract

The article provides an analysis of accuracy indicators for measuring the alcohol by volume (ABV) in vodka performed by various methods according to GOST 32035–2013 «Vodka and Special Vodka. Acceptance Rules and Methods of Anlysis». The results of two rounds of the interlaboratory comparisons on determination of the ABV in vodka conducted to verify the qualifications of accredited testing laboratories are described.

Information is provided on the development of the GSO 11142–2018 reference material for the volume fraction of ethanol in an aqueous solution (VER-2), certified for the volume fraction of ethanol in an aqueous solution, instances of which were used during the interlaboratory comparisons. The conclusion is made about the satisfactory quality of measurements of ABV in vodka in the accredited laboratories.

About the Authors

L. I. Goryaeva
UNIIM – Affiliated Branch of the D. I. Mendeleev Institute for Metrology
Russian Federation

Lyudmila I. Goryaeva – PhD (Chem.), leading researcher 

4 Krasnoarmeyskaya St., Ekaterinburg, 620075



E. K. Fatkulina
UNIIM – Affiliated Branch of the D. I. Mendeleev Institute for Metrology
Russian Federation

Elvira K. Fatkulina – senior engineer 

4 Krasnoarmeyskaya St., Ekaterinburg, 620075



E. P. Shchukina
UNIIM – Affiliated Branch of the D. I. Mendeleev Institute for Metrology
Russian Federation

Eugenia P. Shchukina – engineer 

4 Krasnoarmeyskaya St., Ekaterinburg, 620075

 



References

1. GOST 12712–2013 Vodkas and special vodkas. General specifications. Standartinform Publ., Moscow, 2014. 9 p. (In Russ.).

2. GOST 5962–2013 Rectified ethyl alcohol from edible raw material. Specifications. Standartinform Publ., Moscow, 2014. 8 p. (In Russ.).

3. GOST 33880–2016 Spirits. Terms and definitions. Standartinform Publ., Moscow, 2016. 12 p. (In Russ.).

4. GOST 32098–2013 Vodkas and special vodkas, liqueur and vodka products. Packing, marking, transportation and storage. Standartinform Publ., Moscow, 2014. 9 p. (In Russ.).

5. GOST 32035–2013 Vodkas and special vodkas. Acceptance rules and test methods. Standartinform Publ., Moscow, 2014. 27 p. (In Russ.).

6. GOST 3639–79 Water-alcohol solutions. Methods for the determination of the ethyl alcohol content. IPK Izdatel’stvo standartov Publ., Moscow, 2004. 12 p. (In Russ.).

7. GOST ISO/IEC17025–2019 General requirements for the competence of testing and calibration laboratories. Standartinform Publ., Moscow, 2019. 25 p. (In Russ.).

8. FS.2.1.0036.15 Spirt etilovyi 95%, 96% [Ethyl alcohol 95%, 96%]. In Gosudarstvennaia farmakopeia Rossiiskoi Federatsii [State Pharmacopoeia of the Russian Federation]. XIV edition. 2018. Vol. III. pp. 4804. (In Russ.).

9. GOST R52501–2005 Water for analytical laboratory use. Specifications. Standartinform Publ., Moscow, 2014. 9 p. (In Russ.).

10. GOST 30536–2013 Vodka and ethanol from food raw material. Gas-chromatographic express-method for determination of toxic microadmixtures content. Standartinform Publ., Moscow, 2014. 20 p. (In Russ.).

11. GOST 32036–2013 Ethanol from food raw material. Acceptance rules and test methods. Standartinform Publ., Moscow, 2014. 27 p. (In Russ.).

12. GOST 31685–2012 Ethanol from food raw material. Acceptance rules and test methods. Standartinform Publ., Moscow, 2014. 9 p. (In Russ.).

13. RMG 93-2015 State system for ensuring the uniformity of measurements. Estimation of metrological characteristics of reference materials. Standartinform Publ., Moscow, 2014. 34 p. (In Russ.).

14. GOST ISO Guide 35–2015 Reference materials. General and statistical principles for certification. Standartinform Publ., Moscow, 2016. 59 p. (In Russ.).

15. GOST ISO/IEC17043–2013 Conformity assessment. General requirements for proficiency testing. Standartinform Publ., Moscow, 2016. 32 p. (In Russ.).


Review

For citations:


Goryaeva L.I., Fatkulina E.K., Shchukina E.P. Interlaboratory comparisons on determining of alcohol by volume (abv) in vodka Measurement standards. Measurement Standards. Reference Materials. 2020;16(1):57-66. (In Russ.) https://doi.org/10.20915/2687-0886-2020-16-1-57-66

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ISSN 2687-0886 (Print)