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Development of reference materials for thermodynamic properties: metrological support of measurements in the field of thermal analysisand calorimetry in Russia

https://doi.org/10.20915/2077-1177-2019-15-3-15-22

Abstract

This paper is aimed at analysing the current state and prospects of metrological support and standardisation in the field of thermal analysis in Russia. Main characteristics of reference materials used for testing, graduating, calibrating, and verifying thermal analysis instruments are described.

About the Authors

A. M. Nepomiluev
Ural Research Institute for Metrology
Russian Federation

Andrey M. Nepomiluev – Senior Researcher, Laboratory of Metrology, Thermometry and Surface Density 

4 Krasnoarmeyskaia St., Ekaterinburg, 620075



V. V. Kazantsev
Ural Research Institute for Metrology
Russian Federation

Vyacheslav V. Kazantsev – Ph. D. (Chem.), Sciences, Deputy Director for Scientific Work 

4 Krasnoarmeyskaia St., Ekaterinburg, 620075



A. P. Shipitsyn
Ural Research Institute for Metrology
Russian Federation

Artyom P. Shipitsyn – Engineer, Laboratory of Metrology, Thermometry and Surface Density 

4 Krasnoarmeyskaia St., Ekaterinburg, 620075



References

1. ASTM E 473–16 Standard Terminology Relating to Thermal Analysis and Rheology.

2. GOST R 8.872–214 State verification schedule for means of measuring specific еnthalpy and specific heat of solids in the range of temperature from 700 to 1800 К (In Russ.).

3. Kazantsev V. V., Cherepanov V. I., Sennikova V. N., Averkiev M. V. National primary special standard GET 67–2013 for the units of specific enthalpy and specific heat of solids at temperatures in the 700-1800 K range. Measurement techniques. 2015, No. 2, pp. 11–17. (In Russ.).

4. ASTM E 967–08 Standard Test Method for Temperature Calibration of Differential Scanning Calorimeters and Differential Thermal Analyzers.

5. ISO 11357–1: 2016 Plastics – Differential scanning calorimetry (DSC) – Part 1: General principles.

6. Sabbah R., An Xu-Wu, Chickos J. S., Planas Leita~ o M. L., Roux M. V., Torres L. A. Reference materials for calorimetry and differential thermal analysis. Thermochimica Acta. 1999, vol. 331, pp. 93–204.

7. Gatta G. D., Richardson M. J., Sarge S. M., Stolen S. Standard and calibration and guidelines in microcalorimetry. Part2. Calibration standards for differential scanning calorimetry (IUPAC Technical Report). Pure. Appl. Chem. 2006, vol. 78, № 7, pp. 1455–1476.


Review

For citations:


Nepomiluev A.M., Kazantsev V.V., Shipitsyn A.P. Development of reference materials for thermodynamic properties: metrological support of measurements in the field of thermal analysisand calorimetry in Russia. Measurement Standards. Reference Materials. 2019;15(3):15-22. (In Russ.) https://doi.org/10.20915/2077-1177-2019-15-3-15-22

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ISSN 2687-0886 (Print)