Creating procedures for determining the content of main components in reagents used for synthesizing certified reference materials for composition
https://doi.org/10.20915/10.20915/2077-1177-2017-13-2-27-36
Abstract
Actuality of the research. The need for the development and validation of analysis methods of reagents used for the introduction of elements into reference materials, certified according to the procedure of preparation. The purpose. Development and certification of methods for determining the content of the main component in the reagents used to prepare reference materials. Research methods. Gravimetry, titration, atomic emission spectral analysis with arc excitation, atomic emission spectral analysis with inductively coupled plasma as an excitation source, mass spectral analysis with inductively coupled plasma as ion source. Results. The characteristics of the error of the measurement results are estimated, the Certificates of Attestation of the methods are received, the information is included in the Federal Information Fund.
About the Authors
Margarita A. Dombrovskaya
Ural Federal University named after the first President of Russia B. N. Yeltsin
Russian Federation
Cand. Sci. (Chem.), Associate Professor, Department of Physical and Chemical Analysis, Institute of Physics and Technology, UrFUHead of AFC – Abritration Laboratory for Testing of Nuclear Engineering Materials
Russian Federation
Cand. Sci. (Chem.), Associate Professor, Department of Physical and Chemical Analysis, Institute of Physics and Technology, UrFUHead of AFC – Abritration Laboratory for Testing of Nuclear Engineering Materials
Dmitriy G. Lisienko
Ural Federal University named after the first President of Russia B. N. Yeltsin
Russian Federation
Cand. Sci. (Chem.), Associate Professor, Department of Physical and Chemical Analysis, Institute of Physics and Technology, UrFU, Director of AFC – Abritration Laboratory for Testing of Nuclear Engineering Materials
Russian Federation
Cand. Sci. (Chem.), Associate Professor, Department of Physical and Chemical Analysis, Institute of Physics and Technology, UrFU, Director of AFC – Abritration Laboratory for Testing of Nuclear Engineering Materials
Evgeniya D. Kubrina
Ural Federal University named after the first President of Russia B. N. Yeltsin
Russian Federation
Senior Engineer, Department of Physical and Chemical Analysis, Institute of Physics and Technology, UrFU
Russian Federation
Senior Engineer, Department of Physical and Chemical Analysis, Institute of Physics and Technology, UrFU
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Review
For citations:
Dombrovskaya M.A., Lisienko D.G., Kubrina E.D. Creating procedures for determining the content of main components in reagents used for synthesizing certified reference materials for composition. Measurement Standards. Reference Materials. 2017;13(2):27-36. (In Russ.) https://doi.org/10.20915/10.20915/2077-1177-2017-13-2-27-36
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