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Development ot a black-earth soil reterence material, tested tor fertility indicators

https://doi.org/10.20915/2077-1177-2019-15-4-33-40

Abstract

The authors provide information on the need to develop a reference material (RM) of the southern middle loamy black soil certifiedfor fertility indicators. The information about the stages of RM development is described: selection and preparation of soil material in the field; procedure of averaging soil material.

In the determination of the RM metrological characteristics, the heterogeneity and stability characteristics of the RM are evaluated.

The authors demonstrated the results of the RM certification for agrochemical indicators. The correctness of these results is confirmed by the results obtained in twenty-three accredited laboratories.

The developed RM is registered in the State Register of the Approved Types of Certified Reference Materials under the number GSO 11369-2019-the RMfor composition (of agrochemical indicators) of the southern middle loamy black soil (SACHyuzhP-02).

The RM is intended for metrological support of agroecological monitoring of agroindustrial complex laboratories.

About the Authors

G. A. Stupakova
All-Russian Research Institute o1 Agrochemistry
Russian Federation


E. E. Ignatyeva
All-Russian Research Institute o1 Agrochemistry
Russian Federation


T. I. Shchipletsova
All-Russian Research Institute o1 Agrochemistry
Russian Federation


D. K. Mitrofanov
All-Russian Research Institute o1 Agrochemistry
Russian Federation


References

1. National Atlas of Soils of the Russian Federation, ed. Corresponding Member of RAS S. A. Shoby. Moscow, Astrel. Publ., 2011, pp. 158-159. (In Russ.).

2. Kliushin P. V., Podkolzin 0. A., Marin A. N. Agroecological state of southern chernozems. Agrochemical Herald. 2008. (5):14-15. (In Russ.).

3. Stupakova G. A., Ignatyeva E. E., Pankratova K. G., Shchipletsova T. I., Mitrofanov D. K. Current problems in the metrological supply of tests of technogenically contaminated soils. Collection of reports International scientific and practical conference Actual problems of soil science, ecology and agriculture. Kursk branch of the interregional public organization «Society of soil science to them. V. V. Dokuchaeva». Kursk 2018, pp. 433-437. (In Russ.).

4. Guidelines for the manufacture, research and certification of standard samples of soil composition, ed. academician of the RAS V. G. Sychev. Moscow, VNIIA Publ., 2018, 56 p. (In Russ.).

5. GOST 8.531-2002 State system for ensuring the uniformity of measurements. Reference materials of composition of solid and disperse materials. Ways of homogeneity assessment. Moscow, IPK publishing standards, 2003,12 p. (In Russ.).

6. GOST8.532-2002 State system for ensuring the uniformity of measurements. Certified reference materials of composition of substances and materials. Interlaboratory metrological certification. Content and order of works. Moscow, IPK publishing standards, 2003,10 p. (In Russ.).

7. R50.2.031-2003 State system for ensuring the uniformity of measurements. Reference materials of the composition of substances and materials. Methodology for assessing stability characteristics. Moscow, Gosstandart of Russia, 2003, 10 p. (In Russ.)


Review

For citations:


Stupakova G.A., Ignatyeva E.E., Shchipletsova T.I., Mitrofanov D.K. Development ot a black-earth soil reterence material, tested tor fertility indicators. Measurement Standards. Reference Materials. 2019;15(4):33-40. (In Russ.) https://doi.org/10.20915/2077-1177-2019-15-4-33-40

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ISSN 2687-0886 (Print)