<?xml version="1.0" encoding="UTF-8"?>
<!DOCTYPE article PUBLIC "-//NLM//DTD JATS (Z39.96) Journal Publishing DTD v1.3 20210610//EN" "JATS-journalpublishing1-3.dtd">
<article article-type="research-article" dtd-version="1.3" xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xml:lang="ru"><front><journal-meta><journal-id journal-id-type="publisher-id">rmjournal</journal-id><journal-title-group><journal-title xml:lang="ru">Эталоны. Стандартные  образцы</journal-title><trans-title-group xml:lang="en"><trans-title>Measurement Standards. Reference Materials</trans-title></trans-title-group></journal-title-group><issn pub-type="ppub">2687-0886</issn><publisher><publisher-name>D. I. Mendeleyev Institute for Metrology</publisher-name></publisher></journal-meta><article-meta><article-id pub-id-type="doi">10.20915/2687-0886-2020-16-3-5-21</article-id><article-id custom-type="elpub" pub-id-type="custom">rmjournal-257</article-id><article-categories><subj-group subj-group-type="heading"><subject>Research Article</subject></subj-group><subj-group subj-group-type="section-heading" xml:lang="ru"><subject>Научно-методические подходы и концепции</subject></subj-group><subj-group subj-group-type="section-heading" xml:lang="en"><subject>SCIENTIFIC AND METHODOLOGICAL APPROACHES, CONCEPTS</subject></subj-group></article-categories><title-group><article-title>Прослеживаемость в органическом анализе. Ч. 1: Эквивалентность национальных и международных эталонов</article-title><trans-title-group xml:lang="en"><trans-title>Traceability in organic analysis. Report 1: Equivalence of the national and international measurement standards</trans-title></trans-title-group></title-group><contrib-group><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Михеева</surname><given-names>А. Ю.</given-names></name><name name-style="western" xml:lang="en"><surname>Mikheeva</surname><given-names>A. Yu.</given-names></name></name-alternatives><bio xml:lang="ru"><p>Михеева Алена Юрьевна - кандидат химических наук, ведущий научный сотрудник ФГУП ВНИИМ им. Д. И. Менделеева, ResearcherID B-6506-2019.</p><p>190005, Санкт-Петербург, Московский пр., 19</p></bio><bio xml:lang="en"><p>Alena Yu. Mikheeva - PhD (Chem.), leading researcher, ResearcherID B-6506-2019.</p><p>19 Moskovskiy ave., St. Petersburg, 190005</p></bio><email xlink:type="simple">may@b10.vniim.ru</email><xref ref-type="aff" rid="aff-1"/></contrib><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Крылов</surname><given-names>А. И.</given-names></name><name name-style="western" xml:lang="en"><surname>Krylov</surname><given-names>A. I.</given-names></name></name-alternatives><bio xml:lang="ru"><p>Крылов Анатолий Иванович - доктор химических наук, руководитель отдела госэталонов в области органического и неорганического анализа ФГУП ВНИИМ им. Д.И. Менделеева.</p><p>190005, Санкт-Петербург, Московский пр., 19</p></bio><bio xml:lang="en"><p>Anatoliy I. Krylov - Dr. Sci. (Chem.), head of the department for state measurement standards in the field of organic and inorganic analysis.</p><p>19 Moskovskiy ave., St. Petersburg, 190005</p></bio><email xlink:type="simple">akrylov@b10.vniim.ru</email><xref ref-type="aff" rid="aff-1"/></contrib></contrib-group><aff-alternatives id="aff-1"><aff xml:lang="ru"><institution>ФГУП Всероссийский научно-исследовательский институт метрологии им. Д.И. Менделеева</institution><country>Россия</country></aff><aff xml:lang="en"><institution>D.I. Mendeleyev Institute for Metrology (VNIIM)</institution><country>Russian Federation</country></aff></aff-alternatives><pub-date pub-type="collection"><year>2020</year></pub-date><pub-date pub-type="epub"><day>27</day><month>01</month><year>2021</year></pub-date><volume>16</volume><issue>3</issue><fpage>5</fpage><lpage>21</lpage><permissions><copyright-statement>Copyright &amp;#x00A9; Михеева А.Ю., Крылов А.И., 2021</copyright-statement><copyright-year>2021</copyright-year><copyright-holder xml:lang="ru">Михеева А.Ю., Крылов А.И.</copyright-holder><copyright-holder xml:lang="en">Mikheeva A.Y., Krylov A.I.</copyright-holder><license xml:lang="ru" license-type="creative-commons-attribution" xlink:href="https://creativecommons.org/licenses/by/4.0/" xlink:type="simple"><license-p>Данная работа распространяется под лицензией Creative Commons Attribution 4.0.</license-p></license><license xml:lang="en" license-type="creative-commons-attribution" xlink:href="https://creativecommons.org/licenses/by/4.0/" xlink:type="simple"><license-p>This work is licensed under a Creative Commons Attribution 4.0 License.</license-p></license></permissions><self-uri xlink:href="https://www.rmjournal.ru/jour/article/view/257">https://www.rmjournal.ru/jour/article/view/257</self-uri><abstract><p>В статье рассмотрены вопросы функционирования Международного бюро мер и весов (МБМВ) и соответствующего комитета - Консультативного комитета по количеству вещества (КККВ), координирующего работы по сличениям национальных эталонов в области органического анализа. Описаны структура и задачи КККВ, приведены измерительные категории по количеству вещества. Изложены основные аспекты работы Рабочей группы по органическому анализу (РГОА), детально освещены вопросы систематизации и разделения сличений в области органического анализа, а также различные подходы к формированию областей компетенции на основе ключевых сличений. Подчеркнуто фундаментальное значение чистых органических веществ в обеспечении метрологической прослеживаемости в органическом анализе. Определена ключевая роль Государственного первичного эталона ГЭТ 208 в части подтверждения эквивалентности калибровочных и измерительных возможностей (КИВ) России на международном уровне.</p></abstract><trans-abstract xml:lang="en"><p>The issues of the functioning of the BIPM and the corresponding committee - CCQM, coordinating the work on the comparisons of national standards in the field of organic analysis have considered in this article. The structure and tasks of the CCQM have described and the measurement categories for the amount of substance have given. The main aspects of the OAWG activities have discussed and the issues of systematization and separation of comparisons in the field of organic analysis have discussed in detail and various approaches to the development of competence areas based on key comparisons have set out. The fundamental importance of pure organic substances in providing metrological traceability in organic analysis has highlighted. The key role of the State Primary Standard GET 208 in terms of confirming the equivalence of the calibration and measurement ccapabilities (CMC) of Russia at the international level has been determined.</p></trans-abstract><kwd-group xml:lang="ru"><kwd>стандартный образец</kwd><kwd>сличения</kwd><kwd>сличения национальных эталонов</kwd><kwd>органический анализ</kwd><kwd>метрологическая прослеживаемость</kwd><kwd>международная эквивалентность эталонов</kwd><kwd>эталон</kwd><kwd>калибровка</kwd><kwd>измерения</kwd></kwd-group><kwd-group xml:lang="en"><kwd>reference material</kwd><kwd>comparison</kwd><kwd>national standards comparison</kwd><kwd>organic analysis</kwd><kwd>metrological traceability</kwd><kwd>international standard equivalency</kwd><kwd>standard</kwd><kwd>calibration</kwd><kwd>measurements</kwd></kwd-group></article-meta></front><back><ref-list><title>References</title><ref id="cit1"><label>1</label><citation-alternatives><mixed-citation xml:lang="ru">Documents diplomatic de la Conference du Metre. Paris: Imprimerie nationale, 1875. URL: https://www.bipm.org/utils/common/documents/official/Diplomatic-Conference-Metre.pdf.</mixed-citation><mixed-citation xml:lang="en">Documents diplomatic de la Conference du Metre. Paris: Imprimerie nationale, 1875. Available at: https://www.bipm.org/utils/common/documents/official/Diplomatic-Conference-Metre.pdf.</mixed-citation></citation-alternatives></ref><ref id="cit2"><label>2</label><citation-alternatives><mixed-citation xml:lang="ru">Member States // Bureau International des Poids et Mesures. URL: https://www.bipm.org/en/about-us/member-states.</mixed-citation><mixed-citation xml:lang="en">Member States // Bureau International des Poids et Mesures. Available at: https://www.bipm.org/en/about-us/member-states.</mixed-citation></citation-alternatives></ref><ref id="cit3"><label>3</label><citation-alternatives><mixed-citation xml:lang="ru">Strategic Plan // Bureau international des poids et mesures. URL: https://www.bipm.org/utils/en/pdf/BIPM-strategic-plan.pdf.</mixed-citation><mixed-citation xml:lang="en">Strategic Plan // Bureau International des Poids et Mesures. Available at: https://www.bipm.org/utils/en/pdf/BIPM-strategic-plan.pdf.</mixed-citation></citation-alternatives></ref><ref id="cit4"><label>4</label><citation-alternatives><mixed-citation xml:lang="ru">Compendium of main rules and practices applicable to the BIPM, October 2018. URL: https://www.bipm.org/utils/common/documents/official/compendium.pdf.</mixed-citation><mixed-citation xml:lang="en">Compendium of main rules and practices applicable to the BIPM, October 2018. Available at: https://www.bipm.org/utils/common/documents/official/compendium.pdf.</mixed-citation></citation-alternatives></ref><ref id="cit5"><label>5</label><citation-alternatives><mixed-citation xml:lang="ru">The International System of Units // Bureau International des Poids et Mesures. URL: https://www.bipm.org/en/measurement-units.</mixed-citation><mixed-citation xml:lang="en">The International System of Units // Bureau International des Poids et Mesures. Available at: https://www.bipm.org/en/measurement-units.</mixed-citation></citation-alternatives></ref><ref id="cit6"><label>6</label><citation-alternatives><mixed-citation xml:lang="ru">Международная система единиц. Изд. 9-е. Москва: Росстандарт, 2019. URL: https://www.vniim.ru/files/SI-2019.pdf.</mixed-citation><mixed-citation xml:lang="en">Международная система единиц. Изд. 9-е. Москва: Росстандарт, 2019. Available at: https://www.vniim.ru/files/SI-2019.pdf.</mixed-citation></citation-alternatives></ref><ref id="cit7"><label>7</label><citation-alternatives><mixed-citation xml:lang="ru">The CIPM MRA: 2005 interpretation document. Revised in October 2016 // Bureau International des Poids et Mesures. URL: https://www.bipm.org/utils/common/documents/CIPM-MRA/CIPM-MRA-Interpretation-Document_update2016.pdf.</mixed-citation><mixed-citation xml:lang="en">The CIPM MRA: 2005 interpretation document. Revised in October 2016 // Bureau International des Poids et Mesures. Available at: https://www.bipm.org/utils/common/documents/CIPM-MRA/CIPM-MRA-Interpretation-Document_update2016.pdf.</mixed-citation></citation-alternatives></ref><ref id="cit8"><label>8</label><citation-alternatives><mixed-citation xml:lang="ru">Participating laboratories // Bureau International des Poids et Mesures. URL: https://www.bipm.org/en/cipm-mra/participation.</mixed-citation><mixed-citation xml:lang="en">Participating laboratories // Bureau International des Poids et Mesures. Available at: https://www.bipm.org/en/cipm-mra/participation.</mixed-citation></citation-alternatives></ref><ref id="cit9"><label>9</label><citation-alternatives><mixed-citation xml:lang="ru">KCDB BIPM. URL: https://www.bipm.org/kcdb.</mixed-citation><mixed-citation xml:lang="en">KCDB BIPM. URL: https://www.bipm.org/kcdb.</mixed-citation></citation-alternatives></ref><ref id="cit10"><label>10</label><citation-alternatives><mixed-citation xml:lang="ru">Consultative Committees of the CIPM. URL: https://www.bipm.org/en/committees/cc.</mixed-citation><mixed-citation xml:lang="en">Consultative Committees of the CIPM. Available at: https://www.bipm.org/en/committees/cc.</mixed-citation></citation-alternatives></ref><ref id="cit11"><label>11</label><citation-alternatives><mixed-citation xml:lang="ru">Members. URL: https://www.bipm.org/en/committees/cc/ccqm/members-cc.html.</mixed-citation><mixed-citation xml:lang="en">Members. Available at: https://www.bipm.org/en/committees/cc/ccqm/members-cc.html.</mixed-citation></citation-alternatives></ref><ref id="cit12"><label>12</label><citation-alternatives><mixed-citation xml:lang="ru">CCQM Strategy Document for Rolling Programme Development. Date drafted: 21 February 2017. URL: https://www.bipm.org/utils/en/pdf/CCQM-strategy-document.pdf.</mixed-citation><mixed-citation xml:lang="en">CCQM Strategy Document for Rolling Programme Development. Date drafted: 21 February 2017. Available at: https://www.bipm.org/utils/en/pdf/CCQM-strategy-document.pdf.</mixed-citation></citation-alternatives></ref><ref id="cit13"><label>13</label><citation-alternatives><mixed-citation xml:lang="ru">Traceability exception: delta value isotope ratio measurements. URL: https://www.bipm.org/utils/common/documents/CIPM-MRA/Traceability-Exception-QM1.pdf.</mixed-citation><mixed-citation xml:lang="en">Traceability exception: delta value isotope ratio measurements. Available at: https://www.bipm.org/utils/common/documents/CIPM-MRA/Traceability-Exception-QM1.pdf.</mixed-citation></citation-alternatives></ref><ref id="cit14"><label>14</label><citation-alternatives><mixed-citation xml:lang="ru">Willi A., Brand W. A., Coplen T. B. et al. Assessment of international reference materials for isotope-ratio analysis (IUPAC Technical Report) // Pure and Applied Chemistry. 2014. Voll. 86, Iss. 3. pp. 425-467. https://doi.org/10.1515/pac-2013-1023.</mixed-citation><mixed-citation xml:lang="en">Willi A. Brand, Tyler B. Coplen, Jochen Vogl, Martin Rosner and Thomas Prohaska Assessment of international reference materials for isotope-ratio analysis (IUPAC Technical Report). Pure and Applied Chemistry. 2014;86(3):425-467. https://doi.org/10.1515/pac-2013-1023.</mixed-citation></citation-alternatives></ref><ref id="cit15"><label>15</label><citation-alternatives><mixed-citation xml:lang="ru">CCQM - Consultative Committee for Amount of Substance: Metrology in Chemistry and Biology, CCQM working groups. URL: https://www.bipm.org/en/committees/cc/ccqm/working-groups.html.</mixed-citation><mixed-citation xml:lang="en">CCQM - Consultative Committee for Amount of Substance: Metrology in Chemistry and Biology, CCQM working groups. Available at: https://www.bipm.org/en/committees/cc/ccqm/working-groups.html.</mixed-citation></citation-alternatives></ref><ref id="cit16"><label>16</label><citation-alternatives><mixed-citation xml:lang="ru">list of amount of substance categories, April 2009. URL: https://www.bipm.org/utils/common/pdf/KCDB_2.0/CMC_services/QM_categories.pdf.</mixed-citation><mixed-citation xml:lang="en">list of amount of substance categories, April 2009. Available at: https://www.bipm.org/utils/common/pdf/KCDB_2.0/CMC_services/QM_categories.pdf.</mixed-citation></citation-alternatives></ref><ref id="cit17"><label>17</label><citation-alternatives><mixed-citation xml:lang="ru">CCQM-K5 Final Report, 2001, Key Comparison - Determination of pp’-DDE in Fish Oil. URL: https://www.bipm.org/kcdb/comparison?id=1035.</mixed-citation><mixed-citation xml:lang="en">CCQM-K5 Final Report, 2001, Key Comparison - Determination of pp’-DDE in Fish Oil. Available at: https://www.bipm.org/kcdb/comparison?id=1035.</mixed-citation></citation-alternatives></ref><ref id="cit18"><label>18</label><citation-alternatives><mixed-citation xml:lang="ru">CCQM-K39 Determination of Chlorinated Pesticides in Solution Final Report June 28, 2006. URL: https://www.bipm.org/utils/common/pdf/final_reports/QM/K39/CCQM-K39.pdf.</mixed-citation><mixed-citation xml:lang="en">CCQM-K39, Determination of Chlorinated Pesticides in Solution Final Report June 28, 2006. Available at: https://www.bipm.org/utils/common/pdf/final_reports/QM/K39/CCQM-K39.pdf.</mixed-citation></citation-alternatives></ref><ref id="cit19"><label>19</label><citation-alternatives><mixed-citation xml:lang="ru">CCQM Organic Analysis Working Group Strategy Document, Date drafted: September 2017, Period covered: 2017-2026.</mixed-citation><mixed-citation xml:lang="en">CCQM Organic Analysis Working Group Strategy Document, Date drafted: September 2017, Period covered: 2017-2026.</mixed-citation></citation-alternatives></ref><ref id="cit20"><label>20</label><citation-alternatives><mixed-citation xml:lang="ru">Final report on key comparison CCQM-K55.d (Folic Acid): Mass fraction assignment of folic acid in a high purity material / S. Westwood et al. // Metrologia. 2018. Vol. 55, no.1A. 08013. https://doi.org/10.1088/0026-1394/51/1A/08010.</mixed-citation><mixed-citation xml:lang="en">Westwood S. et al. Final report on key comparison CCQM-K55.c (L-(+)-Valine): Characterization of organic substances for chemical purity. Metrologia. 2014:51(1А):08010. https://doi.org/10.1088/0026-1394/51/1A/08010.</mixed-citation></citation-alternatives></ref><ref id="cit21"><label>21</label><citation-alternatives><mixed-citation xml:lang="ru">Final report on key comparison CCQM-K131: Low-polarity analytes in a multicomponent organic solution: polycyclic aromatic hydrocarbons (PAHs) in acetonitrile/ D. L. Duewer et al. // Metrologia. 2019., Vol. 56, no.1A. 08003. https://doi.org/10.1088/0026-1394/56/1A/08003.</mixed-citation><mixed-citation xml:lang="en">Duewer D. L. et al. Final report on key comparison CCQM-K131: Low-polarity analytes in a multicomponent organic solution: polycyclic aromatic hydrocarbons (PAHs) in acetonitrile. Metrologia. 2019;56(1A):08003. https://doi.org/10.1088/0026-1394/56/1A/08003.</mixed-citation></citation-alternatives></ref><ref id="cit22"><label>22</label><citation-alternatives><mixed-citation xml:lang="ru">Final report on key comparison CCQM-K102: Polybrominated diphenyl ethers in sediment / M. Ricci et al. // Metrologia. 2017. Vol. 54, no.1A. 08026. https://doi.org/10.1088/0026-1394/54/1A/08026.</mixed-citation><mixed-citation xml:lang="en">Ricci M. et al. Final report on key comparison CCQM-K102: Polybrominated diphenyl ethers in sediment. Metrologia. 2017;54(1A):08026. https://doi.org/10.1088/0026-1394/54/1A/08026.</mixed-citation></citation-alternatives></ref><ref id="cit23"><label>23</label><citation-alternatives><mixed-citation xml:lang="ru">High polarity analytes in biological matrix: determination of urea and uric acid in human serum (CCQM-K109)/ Q. Liu et al. // Metrologia. 2019. Vol. 56, no.1A. 08006. https://doi.org/10.1088/0026-1394/56/1A/08006.</mixed-citation><mixed-citation xml:lang="en">Liu Q. et al. High polarity analytes in biological matrix: determination of urea and uric acid in human serum (CCQM-K109)/ // Metrologia. 2019;56(1А):08006. https://doi.org/10.1088/0026-1394/56/1A/08006.</mixed-citation></citation-alternatives></ref><ref id="cit24"><label>24</label><citation-alternatives><mixed-citation xml:lang="ru">Final report on key comparison CCQM-K79: Comparison of value-assigned CRMs and PT materials: Ethanol in aqueous matrix / S. Hein et al. // Metrologia. 2013. Vol. 50, no. 1А. 08005. https://doi.org/10.1088/0026-1394/50/1A/08005.</mixed-citation><mixed-citation xml:lang="en">Hein S. et al. Final report on key comparison CCQM-K79: Comparison of value-assigned CRMs and PT materials: Ethanol in aqueous matrix. Metrologia. 2013;50(1А):08005. https://doi.org/10.1088/0026-1394/50/1A/08005.</mixed-citation></citation-alternatives></ref><ref id="cit25"><label>25</label><citation-alternatives><mixed-citation xml:lang="ru">Final report on key comparison CCQM-K80: Comparison of value-assigned CRMs and PT materials: creatinine in human serum / J. E. Camara et al. URL: https://www.bipm.org/utils/common/pdf/final_reports/QM/K80/CCQM-K80.pdf.</mixed-citation><mixed-citation xml:lang="en">Camara J. E. et al. Final report on key comparison CCQM-K80: Comparison of value-assigned CRMs and PT materials: creatinine in human serum. Available at: https://www.bipm.org/utils/common/pdf/final_reports/QM/K80/CCQM-K80.pdf.</mixed-citation></citation-alternatives></ref><ref id="cit26"><label>26</label><citation-alternatives><mixed-citation xml:lang="ru">Final report on key comparison CCQM-K142: Comparison of CRMs and Value-Assigned Quality Controls: Urea and Uric Acid in Human Serum or Plasma Track A Model 2 Key Comparison // Bureau International des Poids et Mesures. URL: https://www.bipm.org/utils/common/pdf/final_reports/QM/K142/CCQM-K142.pdf.</mixed-citation><mixed-citation xml:lang="en">Final report on key comparison CCQM-K142: Comparison of CRMs and Value-Assigned Quality Controls: Urea and Uric Acid in Human Serum or Plasma Track A Model 2 Key Comparison. Available at: URL: https://www.bipm.org/utils/common/pdf/final_reports/QM/K142/CCQM-K142.pdf.</mixed-citation></citation-alternatives></ref><ref id="cit27"><label>27</label><citation-alternatives><mixed-citation xml:lang="ru">High polarity analytes in food - enrofloxacin and sulfadiazine in bovine tissue. (CCQM-K141) / A. Windust et al. // Metrologia. 2019. Vol. 56, no. 1А. 08005. https://doi.org/10.1088/0026-1394/56/1А/08005.</mixed-citation><mixed-citation xml:lang="en">Windust A. et al. High polarity analytes in food - enrofloxacin and sulfadiazine in bovine tissue. (CCQM-K141). Metrologia. 2019;56(1А):08005. https://doi.org/10.1088/0026-1394/56/1А/08005.</mixed-citation></citation-alternatives></ref><ref id="cit28"><label>28</label><citation-alternatives><mixed-citation xml:lang="ru">Report on key comparison CCQM-K138: determination of aflatoxins (AFB1, AFB2, AFG1, AFG2 and Total AFs) in dried fig / M. Bilsel et al. // Metrologia. 2019. Vol. 56, no. 1A. 08008. https://doi.org/10.1088/0026-1394/56/1A/08008.</mixed-citation><mixed-citation xml:lang="en">Bilsel M. et al. Report on key comparison CCQM-K138: determination of aflatoxins (AFB1, AFB2, AFG1, AFG2 and Total AFs) in dried fig. Metrologia. 2019;56(1А):08008. https://doi.org/10.1088/0026-1394/56/1A/08008.</mixed-citation></citation-alternatives></ref><ref id="cit29"><label>29</label><citation-alternatives><mixed-citation xml:lang="ru">Report B on key comparison CCQM-K133, November 2019: Low-Polarity Analytes in Plastics: Phthalate esters in Polyvinyl Chloride (PVC) // Bureau International des Poids et Mesures. URL: https://www.bipm.org/kcdb/comparison?id=1269.</mixed-citation><mixed-citation xml:lang="en">Report B on key comparison CCQM-K133, November 2019: Low-Polarity Analytes in Plastics: Phthalate esters in Polyvinyl Chloride (PVC). Available at: https://www.bipm.org/kcdb/comparison?id=1269.</mixed-citation></citation-alternatives></ref><ref id="cit30"><label>30</label><citation-alternatives><mixed-citation xml:lang="ru">Final Report on pilot comparison CCQM-P150: Data acquisition and process in qNMR method, October 2016. // Bureau International des Poids et Mesures. URL: https://www.bipm.org/wg/CCQM/OAWG/Restricted/Finalised_Pilot_Study_Reports/OAWG_45.pdf.</mixed-citation><mixed-citation xml:lang="en">Final Report on pilot comparison CCQM-P150: Data acquisition and process in qNMR method, October 2016. Available at: https://www.bipm.org/wg/CCQM/OAWG/Restricted/Finalised_Pilot_Study_Reports/OAWG_45.pdf.</mixed-citation></citation-alternatives></ref><ref id="cit31"><label>31</label><citation-alternatives><mixed-citation xml:lang="ru">Criteria for broad scope claims with the Organic Analysis Working Group (OAWG), Version 2.2, 2019-10-15.</mixed-citation><mixed-citation xml:lang="en">Criteria for broad scope claims with the Organic Analysis Working Group (OAWG), Version 2.2, 2019-10-15.</mixed-citation></citation-alternatives></ref><ref id="cit32"><label>32</label><citation-alternatives><mixed-citation xml:lang="ru">The role of the CCQM OAWG in providing SI traceable calibrators for organic chemical measurements / K. A. Lippa et al. // Accreditation and Quality Assurance. 2019. Vol. 24, pp. 407-415. https://doi.org/10.1007/s00769-019-01407-6.</mixed-citation><mixed-citation xml:lang="en">Lippa K. A. et al. The role of the CCQM OAWG in providing SI traceable calibrators for organic chemical measurements. Accreditation and Quality Assurance. 2019;(24):407-415. https://doi.org/10.1007/s00769-019-01407-6.</mixed-citation></citation-alternatives></ref><ref id="cit33"><label>33</label><citation-alternatives><mixed-citation xml:lang="ru">Об утверждении Государственного первичного эталона единиц массовой (молярной) доли и массовой (молярной) концентрации в жидких и твердых веществах и материалах на основе жидкостной и газовой хромато-масс-спектрометрии с изотопным разбавлением и гравиметрии: Приказ Федерального агентства по техническому регулированию и метрологии (Росстандарт) от 29 января 2015 г. № 125.</mixed-citation><mixed-citation xml:lang="en">On approval of the State primary standard of units of mass (molar) fraction and mass (molar) concentration in liquid and solid substances and materials based on liquid and gas chromatography-mass spectrometry with isotope dilution and gravimetry: Order of the Federal Agency for Technical Regulation and Metrology (Rosstandart) dated January 29, 2015, No. 125.</mixed-citation></citation-alternatives></ref><ref id="cit34"><label>34</label><citation-alternatives><mixed-citation xml:lang="ru">Об обеспечении единства измерений: Федер. закон Рос. Федерации от 26 июня 2008 г. № 102-ФЗ: принят Гос. Думой Федер. Собрания Рос. Федерации 11 июня 2008 г.: одобрен Советом Федерации Федер. Собр. Рос. Федерации 18 июня 2008 г. (в редакции от 27 декабря 2019 г. № 496-ФЗ) // Рос. газета. 2019. 31 декабря.</mixed-citation><mixed-citation xml:lang="en">On ensuring the uniformity of measurements: Feder. the law Ros. Federation of June 26, 2008 No. 102-FZ: adopted by the State. Duma Feder. Collection Ros. Federation June 11, 2008: Approved by the Federation Council Feder. Coll. Grew up. Federation on June 18, 2008 (as amended on December 27, 2019 No. 496-FZ). In: Ros. newspaper. 2019.31 December.</mixed-citation></citation-alternatives></ref><ref id="cit35"><label>35</label><citation-alternatives><mixed-citation xml:lang="ru">Об утверждении Государственной поверочной схемы для средств измерений органических компонентов в жидких и твердых веществах и материалах: Приказ Федерального агентства по техническому регулированию и метрологии (Росстандарт) от 22 мая 2015 г. № 598 // Электронный фонд правовой и нормативно-технической документации.</mixed-citation><mixed-citation xml:lang="en">On approval of the State verification scheme for measuring instruments of organic components in liquid and solid substances and materials: Order of the Federal Agency for Technical Regulation and Metrology (Rosstandart) dated May 22, 2015, No. 598. In: Electronic fund of legal and normative technical documentation.</mixed-citation></citation-alternatives></ref><ref id="cit36"><label>36</label><citation-alternatives><mixed-citation xml:lang="ru">Международный словарь по метрологии: основные и общие понятия и соответствующие термины: пер. с англ. и фр. / Всерос.науч.-исслед. Ин-т метрологии им. Д. И. Менделеева, Белорус. гос. ин-т метрологии. Изд. 2-е, испр. СПб.: НПО «Профессионал», 2010. 82 с.</mixed-citation><mixed-citation xml:lang="en">International vocabulary of metrology: basic and general concepts and related terms: per. from English and fr. Vseross.nauch.-issled. Institute of Metrology. DI. Mendeleev, Belarus. Institute of Metrology. Ed. 2nd, rev. SPb .: NPO «Professional», 2010. 82 p.</mixed-citation></citation-alternatives></ref></ref-list><fn-group><fn fn-type="conflict"><p>The authors declare that there are no conflicts of interest present.</p></fn></fn-group></back></article>
